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Glue and Ovens

Posted: Mon May 05, 2003 10:49 pm
by Paul Tarlow
I think I remember someone posting something about a glue technique for metal to glass that involved using an oven to cure the piece...but I can't remember.

Does anyone remember this?

Thanks,
Paul

glue and heat

Posted: Mon May 05, 2003 11:00 pm
by Ann Demko
I remembered looking through the gallery and finding some pieces by Stacy Street, a fellow Ky. artist, anyway she attached glass to glass with Loctite UV glue and heated it in an oven for 1/2 hr @ 2oo degrees. Don't know why it wouldn't work with metal also. Ann Demko

Posted: Mon May 05, 2003 11:05 pm
by Ron Coleman

Posted: Tue May 06, 2003 11:30 pm
by Lynn Bishop
After a suggestion from someone who had talked to the manufacturer, I started curing mine at 150 degrees for 4 hours...or 28 when I forgot to take them out the previous night. When I try to break off the findings, I find the plating separates from the metal instead of breaking off from the glass or metal. Lynn Bishop

Posted: Wed May 07, 2003 12:36 am
by Paul Tarlow
Does anyone know if this is a Locktite specific technique (the oven thing) or does it work with other epoxy?

Posted: Wed May 07, 2003 6:14 am
by Tony Smith
Most epoxies will work with an accelerated cure by using an elevated temperature... they just don't advertise it. Loctite is an industrial epoxy where the users are concerned about acheiving maximum strength consistently, so they make this information available.

Tony

Posted: Wed May 07, 2003 6:42 am
by Kitty
you can dissolve the epoxy in acetone, and spare yourself the grunt work. sometimes i glue up sterling on earrings and the metal shifts, so the acetone soak overnight takes care of the problem. i'm using 2-Ton by Devcon, and NOT their 5-minute version ... it's nice to have some little jars, like spice jars, around for the acetone treatment. Kitty.

Posted: Wed May 07, 2003 7:46 am
by Paul Tarlow
Tony Smith wrote:Most epoxies will work with an accelerated cure by using an elevated temperature... they just don't advertise it. Loctite is an industrial epoxy where the users are concerned about acheiving maximum strength consistently, so they make this information available.

Tony
So does the elevated temp just speed the process -- or does it make the bond stronger?

Posted: Wed May 07, 2003 8:56 am
by Tony Smith
If you look at the curing curves that are available on the Loctite site under their tech bulletins, http://www.loctite.com/datasheets/tds/H ... E-30cl.pdf
you'll see that epoxy cured at room temperature achieves 100% strength after 24 hours (this is for the E-30CL epoxy that I use). They don't show the curve for the elevated temperature cure, but it achieves 100% strength after 2 to 4 hours.

My guess is that the high temperature cure accomplishes a couple of things: It drives out any moisture or volatiles that might be in the air or on the surface of the glass, and it cures the epoxy thoroughly so that the core of the bondline is as strong as the surface. As with any catalyzed adhesive, thorough mixing is very important.

One other thing to note from the spec sheet is that at elevated temperature, the epoxy loses its strength. At 200°, it only has about 12% strength. So another way to take apart an epoxy joint is to heat it to 200° and pull it apart while hot. It regains this strength when it returns to room temperature, and if held at an elevated temperature for an extended period (>500 hours) it can achieve strength in excess of 150% when returned to room temperature.

Tony

Posted: Wed May 07, 2003 1:03 pm
by Terry Ow-Wing
will this heat method work with the 5 minute epoxy - which is what I have on hand.

Thanks -
Terry O :?:

Posted: Wed May 07, 2003 1:07 pm
by Tony Smith
I believe all Loctite epoxies reference the accelerated cure at temperatures up to 200°... it probably works with other brands as well. It's easy enough to test it and see.

Tony

Posted: Wed May 07, 2003 1:26 pm
by Kitty
Paul -- the heat cure makes the bond substantially stronger. i was having problems with the sterling popping off the glass before i found out about the heat cure. i was so frustrated with the breakdown of the bond, and had been thru so many glues, i finally called Devcon and asked them about it. this was about 2 years ago, and since then i haven't had any more problems, so yeah, it makes a huge difference. Kitty.